Information card for entry 7009716

Structure parameters

• Formula: C66 H66 Ag2 Cl3 O11 P3 Re2
• Calculated formula: C65.78 H65 Ag2 Cl2.34 O11 P3 Re2
• Title of publication: Diastereomeric metallatetrahedron complexes of the type Re2(AgPR3)2(μ-PCy2)(CO)7Z (R = Et and Ph; Z = (−)- and (+)-camphanate): synthesis, structure and CD data
• Authors of publication: Haupt, Hans-Jürgen; Seewald, Oliver; Flörke, Ulrich; Buß, Volker; Weyhermüller, Thomas
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2000
• Journal issue: 16
• Pages of publication: 2837
• a: 14.723 ± 0.008 Å
• b: 16.244 ± 0.004 Å
• c: 16.665 ± 0.004 Å
• α: 98.26 ± 0.01°
• β: 100.47 ± 0.02°
• γ: 101.69 ± 0.02°
• Cell volume: 3770 ± 2 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1678
• Residual factor for significantly intense reflections: 0.0782
• Weighted residual factors for significantly intense reflections: 0.207
• Weighted residual factors for all reflections included in the refinement: 0.2909
• Goodness-of-fit parameter for all reflections included in the refinement: 1.009
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No