Information card for entry 7009797

Structure parameters

• Formula: C20 H31 As Cl Mo O3 P3
• Calculated formula: C20 H31 As Cl Mo O3 P3
• Title of publication: Addition of the [(tBuP)3As]− anion to the cyclopentadienyl ring of [(C5H5)M(CO)3Cl] (M = Mo, W)
• Authors of publication: Bashall, Alan; Hopkins, Alexander D.; Mays, Martin J.; McPartlin, Mary; Wood, Jody A.; Woods, Anthony D.; Wright, Dominic S.
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2000
• Journal issue: 12
• Pages of publication: 1825
• a: 16.308 ± 0.002 Å
• b: 16.303 ± 0.004 Å
• c: 10.132 ± 0.002 Å
• α: 90°
• β: 91 ± 0.013°
• γ: 90°
• Cell volume: 2693.4 ± 0.9 ų
• Cell temperature: 223 ± 2 K
• Ambient diffraction temperature: 223 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0555
• Residual factor for significantly intense reflections: 0.0301
• Weighted residual factors for significantly intense reflections: 0.0635
• Weighted residual factors for all reflections included in the refinement: 0.0732
• Goodness-of-fit parameter for all reflections included in the refinement: 1.031
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No