Information card for entry 7009895

Structure parameters

• Formula: C41 H46 B2 N6 O2 W
• Calculated formula: C41 H43 B2 N6 O2 W
• Title of publication: Hydroboration of metal‒carbon triple bonds †
• Authors of publication: Wadepohl, Hubert; Arnold, Ulrich; Kohl, Ute; Pritzkow, Hans; Wolf, Andreas
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2000
• Journal issue: 20
• Pages of publication: 3554
• a: 19.664 ± 0.011 Å
• b: 8.005 ± 0.005 Å
• c: 26.158 ± 0.016 Å
• α: 90°
• β: 95.63 ± 0.05°
• γ: 90°
• Cell volume: 4098 ± 4 ų
• Cell temperature: 203 ± 2 K
• Ambient diffraction temperature: 203 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/a 1
• Hall space group symbol: -P 2yab
• Residual factor for all reflections: 0.1228
• Residual factor for significantly intense reflections: 0.0584
• Weighted residual factors for significantly intense reflections: 0.1202
• Weighted residual factors for all reflections included in the refinement: 0.1411
• Goodness-of-fit parameter for all reflections included in the refinement: 1.009
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No