Information card for entry 7009896

Structure parameters

• Formula: C34 H41 B2 N6 O2 W
• Calculated formula: C34 H41 B2 N6 O2 W
• Title of publication: Hydroboration of metal‒carbon triple bonds †
• Authors of publication: Wadepohl, Hubert; Arnold, Ulrich; Kohl, Ute; Pritzkow, Hans; Wolf, Andreas
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2000
• Journal issue: 20
• Pages of publication: 3554
• a: 10.308 ± 0.008 Å
• b: 12.342 ± 0.009 Å
• c: 13.508 ± 0.01 Å
• α: 84.29 ± 0.06°
• β: 81 ± 0.06°
• γ: 81.62 ± 0.06°
• Cell volume: 1674 ± 2 ų
• Cell temperature: 203 ± 2 K
• Ambient diffraction temperature: 203 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0373
• Residual factor for significantly intense reflections: 0.0305
• Weighted residual factors for significantly intense reflections: 0.0746
• Weighted residual factors for all reflections included in the refinement: 0.0771
• Goodness-of-fit parameter for all reflections included in the refinement: 1.072
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No