Information card for entry 7010112

Structure parameters

• Formula: C30 H32 Cl2 Cu N6 O18
• Calculated formula: C30 H32 Cl2 Cu N6 O18
• Title of publication: Novel three-dimensional networks cross-linked by two sets of hydrogen bonded frameworks based on 1-D {[M(H2O)4(4,4'-dpdo)][ClO4]2·2(4,4'-dpdo)}n (4,4'-dpdo = 4,4'-bipyridine dioxide; M = Co, Ni, Cu or Zn)
• Authors of publication: Ma, Bao-Qing; Gao, Song; Sun, Hao-Ling; Xu, Guang-Xian
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2001
• Journal issue: 2
• Pages of publication: 130
• a: 5.354 ± 0.0002 Å
• b: 11.8921 ± 0.0004 Å
• c: 15.2705 ± 0.0006 Å
• α: 110.739 ± 0.002°
• β: 94.0425 ± 0.0019°
• γ: 99.235 ± 0.0018°
• Cell volume: 888.91 ± 0.06 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0574
• Residual factor for significantly intense reflections: 0.0421
• Weighted residual factors for significantly intense reflections: 0.1033
• Weighted residual factors for all reflections included in the refinement: 0.1105
• Goodness-of-fit parameter for all reflections included in the refinement: 1.031
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No