Information card for entry 7010179

Structure parameters

• Formula: C53 H43 O20 Os6 Sb2
• Calculated formula: C53 H43 O20 Os6 Sb2
• Title of publication: The reaction of [Os3(μ-H)(CO)10(μ-CO)]− with Ph2SbCl: a cluster with a six-membered Os4Sb2 ring and another with fluxional metal‒metal bonds †
• Authors of publication: Leong, Weng Kee; Chen, Guizhu
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2000
• Journal issue: 23
• Pages of publication: 4442
• a: 14.8356 ± 0.0004 Å
• b: 11.8116 ± 0.0003 Å
• c: 19.4734 ± 0.0004 Å
• α: 90°
• β: 101.587 ± 0.001°
• γ: 90°
• Cell volume: 3342.83 ± 0.14 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 13
• Hermann-Mauguin space group symbol: P 1 2/c 1
• Hall space group symbol: -P 2yc
• Residual factor for all reflections: 0.0506
• Residual factor for significantly intense reflections: 0.0323
• Weighted residual factors for all reflections: 0.0808
• Weighted residual factors for significantly intense reflections: 0.0704
• Goodness-of-fit parameter for all reflections: 1.189
• Goodness-of-fit parameter for significantly intense reflections: 1.164
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No