Information card for entry 7010180

Structure parameters

• Formula: C34.5 H21 Cl O10 Os3 P Sb
• Calculated formula: C34.5 H21 Cl O10 Os3 P Sb
• Title of publication: The reaction of [Os3(μ-H)(CO)10(μ-CO)]− with Ph2SbCl: a cluster with a six-membered Os4Sb2 ring and another with fluxional metal‒metal bonds †
• Authors of publication: Leong, Weng Kee; Chen, Guizhu
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2000
• Journal issue: 23
• Pages of publication: 4442
• a: 12.631 Å
• b: 18.0529 ± 0.0002 Å
• c: 17.1885 ± 0.0001 Å
• α: 90°
• β: 94.469 ± 0.001°
• γ: 90°
• Cell volume: 3907.51 ± 0.05 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0809
• Residual factor for significantly intense reflections: 0.0462
• Weighted residual factors for significantly intense reflections: 0.0857
• Weighted residual factors for all reflections included in the refinement: 0.0983
• Goodness-of-fit parameter for all reflections included in the refinement: 1.068
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No