Crystallography Open Database

Information card for entry 7010181

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Coordinates	7010181.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C37 H27 O10 Os3 Sb2
Calculated formula	C37 H27 O10 Os3 Sb2
Title of publication	The reaction of [Os3(μ-H)(CO)10(μ-CO)]− with Ph2SbCl: a cluster with a six-membered Os4Sb2 ring and another with fluxional metal‒metal bonds †
Authors of publication	Leong, Weng Kee; Chen, Guizhu
Journal of publication	Journal of the Chemical Society, Dalton Transactions
Year of publication	2000
Journal issue	23
Pages of publication	4442
a	13.3803 ± 0.0002 Å
b	17.9495 ± 0.0002 Å
c	17.6996 ± 0.0001 Å
α	90°
β	98.097 ± 0.001°
γ	90°
Cell volume	4208.53 ± 0.08 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.1125
Residual factor for significantly intense reflections	0.0576
Weighted residual factors for significantly intense reflections	0.1212
Weighted residual factors for all reflections included in the refinement	0.149
Goodness-of-fit parameter for all reflections included in the refinement	1.032
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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