Information card for entry 7010192

Structure parameters

• Formula: C24 H19 O14 Os3 P Ru2
• Calculated formula: C24 H19 O14 Os3 P Ru2
• Title of publication: Use of the monocationic fragment [Ru(η5-C5H5)(MeCN)3]+ as an ionic coupling reagent in the synthesis of mixed-metal phosphine clusters †
• Authors of publication: Buntem, Radchada; Gallagher, John F.; Lewis, Jack; Raithby, Paul R.; Rennie, Moira-Ann; Shields, Gregory P.
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2000
• Journal issue: 23
• Pages of publication: 4297
• a: 17.049 ± 0.006 Å
• b: 9.548 ± 0.002 Å
• c: 19.163 ± 0.006 Å
• α: 90°
• β: 94.62 ± 0.03°
• γ: 90°
• Cell volume: 3109.3 ± 1.6 ų
• Cell temperature: 290 ± 2 K
• Ambient diffraction temperature: 290 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0567
• Residual factor for significantly intense reflections: 0.043
• Weighted residual factors for all reflections: 0.1163
• Weighted residual factors for significantly intense reflections: 0.1017
• Goodness-of-fit parameter for all reflections: 1.095
• Goodness-of-fit parameter for significantly intense reflections: 1.082
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No