Information card for entry 7010318

Structure parameters

• Formula: C114 H156 O62 Rh8
• Calculated formula: C114 H142 O62 Rh8
• Title of publication: Dirhodium(II) carboxylate complexes as building blocks. Synthesis and structures of square boxes with tilted walls †
• Authors of publication: Bickley, Jamie F.; Bonar-Law, Richard P.; Femoni, Cristina; MacLean, Elizabeth J.; Steiner, Alexander; Teat, Simon J.
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2000
• Journal issue: 22
• Pages of publication: 4025
• a: 28.749 ± 0.002 Å
• b: 8.5745 ± 0.0007 Å
• c: 40.222 ± 0.003 Å
• α: 90°
• β: 131.477 ± 0.002°
• γ: 90°
• Cell volume: 7428.6 ± 1 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 4
• Space group number: 13
• Hermann-Mauguin space group symbol: P 1 2/c 1
• Hall space group symbol: -P 2yc
• Residual factor for all reflections: 0.1841
• Residual factor for significantly intense reflections: 0.1514
• Weighted residual factors for significantly intense reflections: 0.2936
• Weighted residual factors for all reflections included in the refinement: 0.304
• Goodness-of-fit parameter for all reflections included in the refinement: 1.349
• Diffraction radiation wavelength: 0.6885 Å
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No