Information card for entry 7010319

Structure parameters

• Formula: C120 H154 O57 Rh8
• Calculated formula: C120 H152 O57 Rh8
• SMILES: C12c3ccc(c4ccccc34)C3=[O][Rh]456([O]=C7C(C)(C)Oc8cc(ccc8)OC(C(O4)=[O][Rh]6(O7)(O3)([O]=C(c3ccc(C4=[O][Rh]678(OC9=[O][Rh]8(O4)([O]=C(c4ccc(C8=[O][Rh]%10%11%12([O]=C%13C(C)(C)Oc%14cc(ccc%14)OC(C(O%10)=[O][Rh]%12([O]=C(c%10ccc(C%12=[O][Rh]%14%15([O]=C%16O[Rh]%15(O%12)([O]=2)([O]=C(O%14)C(C)(C)Oc2cccc(c2)OC%16(C)C)[OH]C)(O1)[OH]C)c1c%10cccc1)O%11)(O%13)(O8)[OH]C)(C)C)[OH]C)c1ccccc41)O6)([O]=C(O7)C(C)(C)Oc1cccc(c1)OC9(C)C)[OH]C)[OH]C)c1c3cccc1)O5)[OH]C)(C)C)[OH]C.CO.CO.CO.OC.O.CO.CO.CO.CO
• Title of publication: Dirhodium(II) carboxylate complexes as building blocks. Synthesis and structures of square boxes with tilted walls †
• Authors of publication: Bickley, Jamie F.; Bonar-Law, Richard P.; Femoni, Cristina; MacLean, Elizabeth J.; Steiner, Alexander; Teat, Simon J.
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2000
• Journal issue: 22
• Pages of publication: 4025
• a: 35.1613 ± 0.001 Å
• b: 18.1227 ± 0.0005 Å
• c: 21.5984 ± 0.0006 Å
• α: 90°
• β: 98.216 ± 0.001°
• γ: 90°
• Cell volume: 13621.6 ± 0.7 ų
• Cell temperature: 213 ± 2 K
• Ambient diffraction temperature: 213 ± 2 K
• Number of distinct elements: 4
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.1445
• Residual factor for significantly intense reflections: 0.0959
• Weighted residual factors for significantly intense reflections: 0.2502
• Weighted residual factors for all reflections included in the refinement: 0.2637
• Goodness-of-fit parameter for all reflections included in the refinement: 1.083
• Diffraction radiation wavelength: 0.6855 Å
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No