Information card for entry 7010321

Structure parameters

• Formula: C118 H156 O65 Rh8
• Calculated formula: C118 H154 O65 Rh8
• Title of publication: Dirhodium(II) carboxylate complexes as building blocks. Synthesis and structures of square boxes with tilted walls †
• Authors of publication: Bickley, Jamie F.; Bonar-Law, Richard P.; Femoni, Cristina; MacLean, Elizabeth J.; Steiner, Alexander; Teat, Simon J.
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2000
• Journal issue: 22
• Pages of publication: 4025
• a: 9.5595 ± 0.0012 Å
• b: 20.254 ± 0.003 Å
• c: 20.399 ± 0.003 Å
• α: 95.337 ± 0.017°
• β: 101.8 ± 0.015°
• γ: 94.735 ± 0.017°
• Cell volume: 3828.4 ± 1 ų
• Cell temperature: 213 ± 2 K
• Ambient diffraction temperature: 213 ± 2 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1219
• Residual factor for significantly intense reflections: 0.0628
• Weighted residual factors for significantly intense reflections: 0.163
• Weighted residual factors for all reflections included in the refinement: 0.1822
• Goodness-of-fit parameter for all reflections included in the refinement: 0.848
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No