Information card for entry 7010320

Structure parameters

• Formula: C116 H138 Cl16 O54 Rh8
• Calculated formula: C116 H138 Cl16 O54 Rh8
• Title of publication: Dirhodium(II) carboxylate complexes as building blocks. Synthesis and structures of square boxes with tilted walls †
• Authors of publication: Bickley, Jamie F.; Bonar-Law, Richard P.; Femoni, Cristina; MacLean, Elizabeth J.; Steiner, Alexander; Teat, Simon J.
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2000
• Journal issue: 22
• Pages of publication: 4025
• a: 28.7103 ± 0.0012 Å
• b: 8.6546 ± 0.0004 Å
• c: 30.3073 ± 0.0013 Å
• α: 90°
• β: 93.412 ± 0.001°
• γ: 90°
• Cell volume: 7517.3 ± 0.6 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 13
• Hermann-Mauguin space group symbol: P 1 2/n 1
• Hall space group symbol: -P 2yac
• Residual factor for all reflections: 0.083
• Residual factor for significantly intense reflections: 0.0573
• Weighted residual factors for significantly intense reflections: 0.1389
• Weighted residual factors for all reflections included in the refinement: 0.1463
• Goodness-of-fit parameter for all reflections included in the refinement: 1.04
• Diffraction radiation wavelength: 0.6885 Å
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No