Information card for entry 7010329

Structure parameters

• Common name: Tris(tetraethylammonium) trihydrogendecavanadate dihydrate
• Formula: C24 H67 N3 O30 V10
• Calculated formula: C24 H60 N3 O30 V10
• Title of publication: Hydrogen-bonded aggregates of protonated decavanadate anions in their tetraalkylammonium salts † ‡
• Authors of publication: Nakamura, Setsuko; Ozeki, Tomoji
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2001
• Journal issue: 4
• Pages of publication: 472
• a: 33.4919 ± 0.0009 Å
• b: 21.5128 ± 0.0005 Å
• c: 13.9059 ± 0.0004 Å
• α: 90°
• β: 98.552 ± 0.001°
• γ: 90°
• Cell volume: 9907.9 ± 0.5 ų
• Cell temperature: 298 K
• Ambient diffraction temperature: 298 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.1221
• Residual factor for significantly intense reflections: 0.0587
• Weighted residual factors for significantly intense reflections: 0.1609
• Weighted residual factors for all reflections included in the refinement: 0.1976
• Goodness-of-fit parameter for all reflections included in the refinement: 0.996
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No