Information card for entry 7010330

Structure parameters

• Common name: Bis(tetra-n-propylammonium) tetrahydrogendecavanadate
• Formula: C24 H60 N2 O28 V10
• Calculated formula: C24 H60 N2 O28 V10
• Title of publication: Hydrogen-bonded aggregates of protonated decavanadate anions in their tetraalkylammonium salts † ‡
• Authors of publication: Nakamura, Setsuko; Ozeki, Tomoji
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2001
• Journal issue: 4
• Pages of publication: 472
• a: 8.5568 ± 0.0001 Å
• b: 13.1873 ± 0.0002 Å
• c: 20.1901 ± 0.0003 Å
• α: 90°
• β: 92.653 ± 0.001°
• γ: 90°
• Cell volume: 2275.83 ± 0.06 ų
• Cell temperature: 298 K
• Ambient diffraction temperature: 298 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1016
• Residual factor for significantly intense reflections: 0.0467
• Weighted residual factors for significantly intense reflections: 0.0983
• Weighted residual factors for all reflections included in the refinement: 0.1201
• Goodness-of-fit parameter for all reflections included in the refinement: 0.975
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No