Information card for entry 7010772

Structure parameters

• Formula: C14 H10 N2 O9 Pb
• Calculated formula: C14 H10 N2 O9 Pb
• Title of publication: Synthesis and characterisation of polymeric and oligomeric lead(II) carboxylates
• Authors of publication: Foreman, Mark R. St J.; Plater, M. John; Skakle, Janet M. S.
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2001
• Journal issue: 12
• Pages of publication: 1897
• a: 12.5336 ± 0.0008 Å
• b: 7.1979 ± 0.0005 Å
• c: 18.7487 ± 0.0012 Å
• α: 90°
• β: 102.772 ± 0.001°
• γ: 90°
• Cell volume: 1649.58 ± 0.19 ų
• Cell temperature: 298 ± 2 K
• Ambient diffraction temperature: 298 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1113
• Residual factor for significantly intense reflections: 0.0445
• Weighted residual factors for significantly intense reflections: 0.0623
• Weighted residual factors for all reflections included in the refinement: 0.0738
• Goodness-of-fit parameter for all reflections included in the refinement: 0.848
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No