Information card for entry 7010773

Structure parameters

• Formula: C14 H8 N4 O13 Pb
• Calculated formula: C14 H8 N4 O13 Pb
• Title of publication: Synthesis and characterisation of polymeric and oligomeric lead(II) carboxylates
• Authors of publication: Foreman, Mark R. St J.; Plater, M. John; Skakle, Janet M. S.
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2001
• Journal issue: 12
• Pages of publication: 1897
• a: 7.2864 ± 0.0003 Å
• b: 11.0392 ± 0.0005 Å
• c: 23.201 ± 0.0011 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 1866.2 ± 0.14 ų
• Cell temperature: 298 ± 2 K
• Ambient diffraction temperature: 298 ± 2 K
• Number of distinct elements: 5
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.0347
• Residual factor for significantly intense reflections: 0.0251
• Weighted residual factors for significantly intense reflections: 0.0418
• Weighted residual factors for all reflections included in the refinement: 0.0434
• Goodness-of-fit parameter for all reflections included in the refinement: 0.929
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No