Information card for entry 7010779

Structure parameters

• Formula: C33 H57 Cl4 Li N2 O2 Si2 Zr
• Calculated formula: C33 H52 Cl4 Li N2 O2 Si2 Zr
• Title of publication: The reactions of lithium trimethysilylmethyls with isocyanides; structures and reactions of the derived lithium 1-azaallyls, β-diketiminates and a 1-azabuta-1,3-dienyl-3-amide
• Authors of publication: Hitchcock, Peter B.; Lappert, Michael F.; Layh, Marcus
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2001
• Journal issue: 16
• Pages of publication: 2409
• a: 14.838 ± 0.003 Å
• b: 15.446 ± 0.003 Å
• c: 19.174 ± 0.004 Å
• α: 90°
• β: 105.05 ± 0.02°
• γ: 90°
• Cell volume: 4243.7 ± 1.5 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0586
• Residual factor for significantly intense reflections: 0.0403
• Weighted residual factors for all reflections: 0.1045
• Weighted residual factors for significantly intense reflections: 0.0939
• Goodness-of-fit parameter for all reflections: 1.019
• Goodness-of-fit parameter for significantly intense reflections: 1.046
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No