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Information card for entry 7010781
Preview
Coordinates | 7010781.cif |
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Original paper (by DOI) | HTML |
Formula | C34 H49 Li N4 Si |
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Calculated formula | C34 H49 Li N4 Si |
SMILES | [Li]12([N](=C([Si](C)(C)C)C(=C\c3ccccc3)/N1c1c(cccc1C)C)c1c(cccc1C)C)[N](CC[N]2(C)C)(C)C |
Title of publication | The reactions of lithium trimethysilylmethyls with isocyanides; structures and reactions of the derived lithium 1-azaallyls, β-diketiminates and a 1-azabuta-1,3-dienyl-3-amide |
Authors of publication | Hitchcock, Peter B.; Lappert, Michael F.; Layh, Marcus |
Journal of publication | Journal of the Chemical Society, Dalton Transactions |
Year of publication | 2001 |
Journal issue | 16 |
Pages of publication | 2409 |
a | 10.887 ± 0.003 Å |
b | 11.272 ± 0.002 Å |
c | 14.266 ± 0.003 Å |
α | 87.11 ± 0.02° |
β | 76.64 ± 0.02° |
γ | 84.46 ± 0.02° |
Cell volume | 1694.6 ± 0.7 Å3 |
Cell temperature | 173 ± 2 K |
Ambient diffraction temperature | 173 ± 2 K |
Number of distinct elements | 5 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.1075 |
Residual factor for significantly intense reflections | 0.0629 |
Weighted residual factors for all reflections | 0.1781 |
Weighted residual factors for significantly intense reflections | 0.1486 |
Goodness-of-fit parameter for all reflections | 1.038 |
Goodness-of-fit parameter for significantly intense reflections | 1.104 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7010781.html
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