Information card for entry 7010811

Structure parameters

• Formula: C21 H17 F18 O9 Sm
• Calculated formula: C21 H17 F18 O9 Sm
• Title of publication: Reactivity of the europium hexafluoroacetylacetonate (hfac) complex, Eu(hfac)3(diglyme), and related analogs with potassium: formation of the fluoride hfac “ate” complexes, [LnF(hfac)3K(diglyme)]2
• Authors of publication: William J. Evans; Dimitrios G. Giarikos; Matthew A. Johnston; Michael A. Greci; Joseph W. Ziller
• Journal of publication: J. Chem. Soc., Dalton Trans.
• Year of publication: 2002
• Journal issue: 4
• Pages of publication: 520 - 526
• a: 10.121 ± 0.0006 Å
• b: 15.6745 ± 0.001 Å
• c: 19.301 ± 0.0012 Å
• α: 90°
• β: 97.248 ± 0.001°
• γ: 90°
• Cell volume: 3037.5 ± 0.3 ų
• Cell temperature: 158 ± 2 K
• Ambient diffraction temperature: 158 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.022
• Residual factor for significantly intense reflections: 0.019
• Weighted residual factors for significantly intense reflections: 0.0481
• Weighted residual factors for all reflections included in the refinement: 0.0497
• Goodness-of-fit parameter for all reflections included in the refinement: 1.029
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No