Information card for entry 7010812

Structure parameters

• Formula: C42 H34 F38 K2 O18 Sm2
• Calculated formula: C42 H34 F38 K2 O18 Sm2
• Title of publication: Reactivity of the europium hexafluoroacetylacetonate (hfac) complex, Eu(hfac)3(diglyme), and related analogs with potassium: formation of the fluoride hfac “ate” complexes, [LnF(hfac)3K(diglyme)]2
• Authors of publication: William J. Evans; Dimitrios G. Giarikos; Matthew A. Johnston; Michael A. Greci; Joseph W. Ziller
• Journal of publication: J. Chem. Soc., Dalton Trans.
• Year of publication: 2002
• Journal issue: 4
• Pages of publication: 520 - 526
• a: 12.0241 ± 0.0006 Å
• b: 12.4246 ± 0.0006 Å
• c: 13.5664 ± 0.0007 Å
• α: 92.292 ± 0.001°
• β: 114.633 ± 0.001°
• γ: 113.686 ± 0.001°
• Cell volume: 1633.89 ± 0.14 ų
• Cell temperature: 163 ± 2 K
• Ambient diffraction temperature: 163 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0269
• Residual factor for significantly intense reflections: 0.0247
• Weighted residual factors for significantly intense reflections: 0.0614
• Weighted residual factors for all reflections included in the refinement: 0.0628
• Goodness-of-fit parameter for all reflections included in the refinement: 1.026
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No