Information card for entry 7011008

Structure parameters

• Formula: C34.5 H50 Cl4 F6 Fe N3 O2 Sb
• Calculated formula: C34.5 H45 Cl4 F6 Fe N3 O2 Sb
• Title of publication: Cationic 2,6-bis(imino)pyridine iron and cobalt complexes: synthesis, structures, ethylene polymerisation and ethylene/polar monomer co-polymerisation studies
• Authors of publication: George J. P. Britovsek; Vernon C. Gibson; Stefan K. Spitzmesser; Kilian P. Tellmann; Andrew J. P. White; David J. Williams
• Journal of publication: J. Chem. Soc., Dalton Trans.
• Year of publication: 2002
• Journal issue: 6
• Pages of publication: 1159 - 1171
• a: 10.075 ± 0.002 Å
• b: 13.265 ± 0.003 Å
• c: 18.925 ± 0.003 Å
• α: 84.223 ± 0.015°
• β: 78.89 ± 0.02°
• γ: 68.341 ± 0.015°
• Cell volume: 2305.4 ± 0.8 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1711
• Residual factor for significantly intense reflections: 0.082
• Weighted residual factors for all reflections: 0.2485
• Weighted residual factors for significantly intense reflections: 0.1854
• Goodness-of-fit parameter for all reflections: 1.031
• Goodness-of-fit parameter for significantly intense reflections: 1.175
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No