Information card for entry 7011009

Structure parameters

• Formula: C40 H54 Cl4 F6 Fe N3 O2 Sb
• Calculated formula: C40 H52 Cl4 F6 Fe N3 O2 Sb
• Title of publication: Cationic 2,6-bis(imino)pyridine iron and cobalt complexes: synthesis, structures, ethylene polymerisation and ethylene/polar monomer co-polymerisation studies
• Authors of publication: George J. P. Britovsek; Vernon C. Gibson; Stefan K. Spitzmesser; Kilian P. Tellmann; Andrew J. P. White; David J. Williams
• Journal of publication: J. Chem. Soc., Dalton Trans.
• Year of publication: 2002
• Journal issue: 6
• Pages of publication: 1159 - 1171
• a: 15.005 ± 0.002 Å
• b: 16.903 ± 0.002 Å
• c: 18.815 ± 0.002 Å
• α: 90°
• β: 94.95 ± 0.009°
• γ: 90°
• Cell volume: 4754.2 ± 1 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1253
• Residual factor for significantly intense reflections: 0.0656
• Weighted residual factors for all reflections: 0.192
• Weighted residual factors for significantly intense reflections: 0.1513
• Goodness-of-fit parameter for all reflections: 1.003
• Goodness-of-fit parameter for significantly intense reflections: 1.104
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No