Information card for entry 7011026

Structure parameters

• Formula: C51.5 H65 Cl0.5 F9 N4 O1.5 P3.5 Pd2
• Calculated formula: C51.5 H56 Cl0.5 F9 N4 O1.5 P3.5 Pd2
• Title of publication: Synthesis of bis[palladium(II)] and bis[platinum(II)] complexes containing chiral, linear quadridentate ligands with a P2N2 donor set
• Authors of publication: Justine Bennett; A. David Rae; Geoffrey Salem; Natalie C. Ward; Paul Waring; Kerri Wells; Anthony C. Willis
• Journal of publication: J. Chem. Soc., Dalton Trans.
• Year of publication: 2002
• Journal issue: 2
• Pages of publication: 234 - 243
• a: 17.622 ± 0.004 Å
• b: 21.207 ± 0.003 Å
• c: 16.001 ± 0.003 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 5980 ± 2 ų
• Cell temperature: 193.2 K
• Ambient diffraction temperature: 193.2 K
• Number of distinct elements: 8
• Space group number: 18
• Hermann-Mauguin space group symbol: P 21 21 2
• Hall space group symbol: P 2 2ab
• Residual factor for all reflections: 0.076
• Residual factor for significantly intense reflections: 0.06
• Weighted residual factors for all reflections: 0.096
• Weighted residual factors for all reflections included in the refinement: 0.093
• Goodness-of-fit parameter for all reflections: 1.396
• Goodness-of-fit parameter for all reflections included in the refinement: 1.463
• Diffraction radiation wavelength: 1.5418 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No