Information card for entry 7011027

Structure parameters

• Formula: C31 H65 As Li6 N6
• Calculated formula: C31.02 H67.86 As Li6 N6
• Title of publication: Synthesis, structures and coordination behaviour of [As(NR)3]3− trianions
• Authors of publication: Allan Bashall; Andrew D. Bond; Alexander D. Hopkins; Sara J. Kidd; Mary McPartlin; Alexander Steiner; Robert Wolf; Anthony D. Woods; Dominic S. Wright
• Journal of publication: J. Chem. Soc., Dalton Trans.
• Year of publication: 2002
• Journal issue: 3
• Pages of publication: 343 - 351
• a: 16.0568 ± 0.0012 Å
• b: 16.0568 ± 0.0012 Å
• c: 13.5862 ± 0.0012 Å
• α: 90°
• β: 90°
• γ: 120°
• Cell volume: 3033.5 ± 0.4 ų
• Cell temperature: 180 ± 2 K
• Ambient diffraction temperature: 180 ± 2 K
• Number of distinct elements: 5
• Space group number: 166
• Hermann-Mauguin space group symbol: R -3 m :H
• Hall space group symbol: -R 3 2"
• Residual factor for all reflections: 0.072
• Residual factor for significantly intense reflections: 0.0646
• Weighted residual factors for significantly intense reflections: 0.1646
• Weighted residual factors for all reflections included in the refinement: 0.1699
• Goodness-of-fit parameter for all reflections included in the refinement: 1.146
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No