Information card for entry 7011029

Structure parameters

• Formula: C30 H63 As7 Li3 N3 O3
• Calculated formula: C30 H63 As7 Li3 N3 O3
• Title of publication: Synthesis, structures and coordination behaviour of [As(NR)3]3− trianions
• Authors of publication: Allan Bashall; Andrew D. Bond; Alexander D. Hopkins; Sara J. Kidd; Mary McPartlin; Alexander Steiner; Robert Wolf; Anthony D. Woods; Dominic S. Wright
• Journal of publication: J. Chem. Soc., Dalton Trans.
• Year of publication: 2002
• Journal issue: 3
• Pages of publication: 343 - 351
• a: 11.3301 ± 0.0003 Å
• b: 14.5022 ± 0.0005 Å
• c: 15.8403 ± 0.0006 Å
• α: 116.203 ± 0.002°
• β: 98.386 ± 0.002°
• γ: 103.745 ± 0.002°
• Cell volume: 2172.48 ± 0.14 ų
• Cell temperature: 180 ± 2 K
• Ambient diffraction temperature: 180 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0664
• Residual factor for significantly intense reflections: 0.042
• Weighted residual factors for significantly intense reflections: 0.0846
• Weighted residual factors for all reflections included in the refinement: 0.0933
• Goodness-of-fit parameter for all reflections included in the refinement: 1.034
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No