Information card for entry 7011030

Structure parameters

• Formula: C72 H98 As2 Li8 N16 O8
• Calculated formula: C72 H98 As2 Li8 N16 O8
• Title of publication: Synthesis, structures and coordination behaviour of [As(NR)3]3− trianions
• Authors of publication: Allan Bashall; Andrew D. Bond; Alexander D. Hopkins; Sara J. Kidd; Mary McPartlin; Alexander Steiner; Robert Wolf; Anthony D. Woods; Dominic S. Wright
• Journal of publication: J. Chem. Soc., Dalton Trans.
• Year of publication: 2002
• Journal issue: 3
• Pages of publication: 343 - 351
• a: 11.8168 ± 0.0006 Å
• b: 13.209 ± 0.0006 Å
• c: 14.3578 ± 0.0005 Å
• α: 82.657 ± 0.003°
• β: 71.871 ± 0.003°
• γ: 69.363 ± 0.002°
• Cell volume: 1992.75 ± 0.16 ų
• Cell temperature: 180 ± 2 K
• Ambient diffraction temperature: 180 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0633
• Residual factor for significantly intense reflections: 0.0485
• Weighted residual factors for significantly intense reflections: 0.1141
• Weighted residual factors for all reflections included in the refinement: 0.1204
• Goodness-of-fit parameter for all reflections included in the refinement: 1.042
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No