Crystallography Open Database

Information card for entry 7011235

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Coordinates	7011235.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C28 H25 Cl3 N O P Pd
Calculated formula	C28 H25 Cl3 N O P Pd
Title of publication	Ligand effects on palladium complex catalyzed copolymerization of ethylene/carbon monoxide
Authors of publication	Reddy, K. Rajender; Tsai, Wei-Wen; Surekha, K.; Lee, Gene-Hsiang; Peng, Shie-Ming; Chen, Jwu-Ting; Liu, Shiuh-Tzung
Journal of publication	Journal of the Chemical Society, Dalton Transactions
Year of publication	2002
Journal issue	8
Pages of publication	1776
a	9.5745 ± 0.0001 Å
b	9.8728 ± 0.0001 Å
c	15.3826 ± 0.0002 Å
α	79.672 ± 0.001°
β	83.546 ± 0.001°
γ	81.263 ± 0.001°
Cell volume	1408.48 ± 0.03 Å³
Cell temperature	295 ± 2 K
Ambient diffraction temperature	295 ± 2 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0534
Residual factor for significantly intense reflections	0.0372
Weighted residual factors for significantly intense reflections	0.0789
Weighted residual factors for all reflections included in the refinement	0.0849
Goodness-of-fit parameter for all reflections included in the refinement	1.071
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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