Information card for entry 7011236

Structure parameters

• Formula: C26 H25 Cl N O P Pd
• Calculated formula: C26 H25 Cl N O P Pd
• Title of publication: Ligand effects on palladium complex catalyzed copolymerization of ethylene/carbon monoxide
• Authors of publication: Reddy, K. Rajender; Tsai, Wei-Wen; Surekha, K.; Lee, Gene-Hsiang; Peng, Shie-Ming; Chen, Jwu-Ting; Liu, Shiuh-Tzung
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2002
• Journal issue: 8
• Pages of publication: 1776
• a: 8.9142 ± 0.0002 Å
• b: 10.3657 ± 0.0002 Å
• c: 14.4963 ± 0.0003 Å
• α: 103.052 ± 0.001°
• β: 101.345 ± 0.001°
• γ: 92.264 ± 0.001°
• Cell volume: 1274.44 ± 0.05 ų
• Cell temperature: 295 ± 2 K
• Ambient diffraction temperature: 295 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0761
• Residual factor for significantly intense reflections: 0.0503
• Weighted residual factors for significantly intense reflections: 0.1119
• Weighted residual factors for all reflections included in the refinement: 0.1233
• Goodness-of-fit parameter for all reflections included in the refinement: 1.137
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No