Information card for entry 7011539

Structure parameters

• Formula: C32 H38 Cl2 N2 O4 P Rh S3
• Calculated formula: C32 H38 Cl2 N2 O4 P Rh S3
• Title of publication: Reactivity of Rh(i) and Rh(iii) complexes containing a PNO hydrazonic ligand toward HCl
• Authors of publication: Pelagatti, Paolo; Bacchi, Alessia; Bobbio, Carla; Carcelli, Mauro; Costa, Mirco; Fochi, Andrea; Pelizzi, Corrado
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2002
• Journal issue: 8
• Pages of publication: 1820
• a: 13.939 ± 0.005 Å
• b: 12.862 ± 0.005 Å
• c: 20.133 ± 0.005 Å
• α: 90°
• β: 92.1 ± 0.05°
• γ: 90°
• Cell volume: 3607 ± 2 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0871
• Residual factor for significantly intense reflections: 0.0606
• Weighted residual factors for significantly intense reflections: 0.1728
• Weighted residual factors for all reflections included in the refinement: 0.1973
• Goodness-of-fit parameter for all reflections included in the refinement: 0.934
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No