Information card for entry 7011540

Structure parameters

• Formula: C29 H26 Cl3.6 I0.4 N2 O2 P Rh
• Calculated formula: C29 H26 Cl3.569 I0.431 N2 O2 P Rh
• Title of publication: Reactivity of Rh(i) and Rh(iii) complexes containing a PNO hydrazonic ligand toward HCl
• Authors of publication: Pelagatti, Paolo; Bacchi, Alessia; Bobbio, Carla; Carcelli, Mauro; Costa, Mirco; Fochi, Andrea; Pelizzi, Corrado
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2002
• Journal issue: 8
• Pages of publication: 1820
• a: 18.172 ± 0.005 Å
• b: 22.005 ± 0.005 Å
• c: 14.952 ± 0.005 Å
• α: 90 ± 0°
• β: 90 ± 0°
• γ: 90 ± 0°
• Cell volume: 5979 ± 3 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 8
• Space group number: 61
• Hermann-Mauguin space group symbol: P b c a
• Hall space group symbol: -P 2ac 2ab
• Residual factor for all reflections: 0.2232
• Residual factor for significantly intense reflections: 0.0422
• Weighted residual factors for significantly intense reflections: 0.0738
• Weighted residual factors for all reflections included in the refinement: 0.0967
• Goodness-of-fit parameter for all reflections included in the refinement: 0.578
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No