Information card for entry 7012181

Structure parameters

• Formula: C41.5 H17 Cl3 Co8 O22 Si4
• Calculated formula: C41.5 H17 Cl3 Co8 O22 Si4
• Title of publication: The preparation and characterisation of monomeric and linked metal carbonyl clusters containing the closo-Si2Co4 pseudo-octahedral core
• Authors of publication: Evans, Cameron; Harfoot, Gwion J.; Scott McIndoe, J.; John McAdam, C.; Mackay, Kenneth M.; Nicholson, Brian K.; Robinson, Brian H.; Van Tiel, Martin L.
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2002
• Journal issue: 24
• Pages of publication: 4678
• a: 9.323 ± 0.004 Å
• b: 18.192 ± 0.007 Å
• c: 16.89 ± 0.007 Å
• α: 90°
• β: 103.34 ± 0.005°
• γ: 90°
• Cell volume: 2787 ± 2 ų
• Cell temperature: 158 ± 2 K
• Ambient diffraction temperature: 158 ± 2 K
• Number of distinct elements: 6
• Space group number: 4
• Hermann-Mauguin space group symbol: P 1 21 1
• Hall space group symbol: P 2yb
• Residual factor for all reflections: 0.1021
• Residual factor for significantly intense reflections: 0.0469
• Weighted residual factors for significantly intense reflections: 0.1001
• Weighted residual factors for all reflections included in the refinement: 0.1108
• Goodness-of-fit parameter for all reflections included in the refinement: 1.02
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No