Information card for entry 7012182

Structure parameters

• Formula: C26.5 H14 Co4 O11 Si2
• Calculated formula: C26.5 H10 Co4 O11 Si2
• Title of publication: The preparation and characterisation of monomeric and linked metal carbonyl clusters containing the closo-Si2Co4 pseudo-octahedral core
• Authors of publication: Evans, Cameron; Harfoot, Gwion J.; Scott McIndoe, J.; John McAdam, C.; Mackay, Kenneth M.; Nicholson, Brian K.; Robinson, Brian H.; Van Tiel, Martin L.
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2002
• Journal issue: 24
• Pages of publication: 4678
• a: 9.46 ± 0.01 Å
• b: 21.58 ± 0.01 Å
• c: 14.85 ± 0.01 Å
• α: 90°
• β: 90.09 ± 0.01°
• γ: 90°
• Cell volume: 3032 ± 4 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0499
• Residual factor for significantly intense reflections: 0.0365
• Weighted residual factors for significantly intense reflections: 0.0888
• Weighted residual factors for all reflections included in the refinement: 0.0958
• Goodness-of-fit parameter for all reflections included in the refinement: 1.048
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No