Information card for entry 7012271

Structure parameters

• Formula: C26 H43 F6 N4 Ni2 O7 P
• Calculated formula: C26 H43 F6 N4 Ni2 O7 P
• Title of publication: Dinuclear nickel(ii) complexes of reduced asymmetric compartmental ligandsIn memoriam Noel McAuliffe (1941‒2002).
• Authors of publication: Adams, Harry; Clunas, Scott; Fenton, David E.; Spey, Sharon E.
• Journal of publication: Dalton Transactions
• Year of publication: 2003
• Journal issue: 4
• Pages of publication: 625
• a: 11.771 ± 0.002 Å
• b: 16.086 ± 0.003 Å
• c: 17.687 ± 0.003 Å
• α: 90°
• β: 103.915 ± 0.004°
• γ: 90°
• Cell volume: 3250.7 ± 1 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1892
• Residual factor for significantly intense reflections: 0.0613
• Weighted residual factors for significantly intense reflections: 0.1241
• Weighted residual factors for all reflections included in the refinement: 0.1589
• Goodness-of-fit parameter for all reflections included in the refinement: 0.826
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No