Information card for entry 7012272

Structure parameters

• Formula: C52 H88 F12 N8 Ni4 O15 P2
• Calculated formula: C52 H84 F12 N8 Ni4 O15 P2
• Title of publication: Dinuclear nickel(ii) complexes of reduced asymmetric compartmental ligandsIn memoriam Noel McAuliffe (1941‒2002).
• Authors of publication: Adams, Harry; Clunas, Scott; Fenton, David E.; Spey, Sharon E.
• Journal of publication: Dalton Transactions
• Year of publication: 2003
• Journal issue: 4
• Pages of publication: 625
• a: 20.653 ± 0.006 Å
• b: 10.707 ± 0.003 Å
• c: 31.627 ± 0.009 Å
• α: 90°
• β: 92.049 ± 0.005°
• γ: 90°
• Cell volume: 6989 ± 3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.2149
• Residual factor for significantly intense reflections: 0.0629
• Weighted residual factors for significantly intense reflections: 0.131
• Weighted residual factors for all reflections included in the refinement: 0.1702
• Goodness-of-fit parameter for all reflections included in the refinement: 0.803
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No