Information card for entry 7012379

Structure parameters

• Formula: C55 H92 Li2 N2 O6 Zn2
• Calculated formula: C55 H92 Li2 N2 O6 Zn2
• Title of publication: New motifs in lithium zincate chemistry: a solid-state structural study of PhC(O)N(R)ZnR'2Li·2thf (R, R' = alkyl, aryl) and [PhC(O)N(Ph)Li·thf]·[PhC(O)N(Ph)Zn(But)2Li·thf]
• Authors of publication: Boss, Sally R.; Haigh, Robert; Linton, David J.; Schooler, Paul; Shields, Gregory P.; Wheatley, Andrew E. H.
• Journal of publication: Dalton Transactions
• Year of publication: 2003
• Journal issue: 5
• Pages of publication: 1001
• a: 15.0541 ± 0.0003 Å
• b: 17.0524 ± 0.0004 Å
• c: 23.75 ± 0.0005 Å
• α: 90°
• β: 96.626 ± 0.002°
• γ: 90°
• Cell volume: 6056.1 ± 0.2 ų
• Cell temperature: 180 ± 2 K
• Ambient diffraction temperature: 180 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1145
• Residual factor for significantly intense reflections: 0.0673
• Weighted residual factors for significantly intense reflections: 0.1559
• Weighted residual factors for all reflections included in the refinement: 0.1835
• Goodness-of-fit parameter for all reflections included in the refinement: 1.018
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No