Information card for entry 7012380

Structure parameters

• Formula: C205 H260 Li8 N8 O16.5 Zn4
• Calculated formula: C205.5 H216 Li8 N8 O16 Zn4
• Title of publication: New motifs in lithium zincate chemistry: a solid-state structural study of PhC(O)N(R)ZnR'2Li·2thf (R, R' = alkyl, aryl) and [PhC(O)N(Ph)Li·thf]·[PhC(O)N(Ph)Zn(But)2Li·thf]
• Authors of publication: Boss, Sally R.; Haigh, Robert; Linton, David J.; Schooler, Paul; Shields, Gregory P.; Wheatley, Andrew E. H.
• Journal of publication: Dalton Transactions
• Year of publication: 2003
• Journal issue: 5
• Pages of publication: 1001
• a: 21.937 ± 0.004 Å
• b: 24.142 ± 0.005 Å
• c: 24.51 ± 0.005 Å
• α: 72.69 ± 0.03°
• β: 87.39 ± 0.03°
• γ: 64.56 ± 0.03°
• Cell volume: 11140 ± 5 ų
• Cell temperature: 230 ± 2 K
• Ambient diffraction temperature: 230 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1484
• Residual factor for significantly intense reflections: 0.0949
• Weighted residual factors for significantly intense reflections: 0.2549
• Weighted residual factors for all reflections included in the refinement: 0.2991
• Goodness-of-fit parameter for all reflections included in the refinement: 1.03
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No