Information card for entry 7012488

Structure parameters

• Formula: C27 H33 N3 Pb Si2
• Calculated formula: C27 H33 N3 Pb Si2
• SMILES: [Pb]12[n]3c(cccc3C=C(N1[Si](C)(C)C)c1ccccc1)C=C(N2[Si](C)(C)C)c1ccccc1
• Title of publication: Synthesis and structural characterisation of low-valent Group 14 metal complexes containing tridentate 2,6-pyridyl-bridged bis(1-azaallyl) ligands
• Authors of publication: Leung, Wing-Por; Hou, Henry L.; Cheng, Hui; Yang, Qing-Chuan; Li, Hung-Wing; Mak, Thomas C. W.
• Journal of publication: Dalton Transactions
• Year of publication: 2003
• Journal issue: 8
• Pages of publication: 1505
• a: 8.5695 ± 0.0012 Å
• b: 11.7207 ± 0.0016 Å
• c: 13.8504 ± 0.0019 Å
• α: 84.487 ± 0.002°
• β: 83.495 ± 0.003°
• γ: 87.398 ± 0.003°
• Cell volume: 1375 ± 0.3 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0291
• Residual factor for significantly intense reflections: 0.0246
• Weighted residual factors for significantly intense reflections: 0.0578
• Weighted residual factors for all reflections included in the refinement: 0.0588
• Goodness-of-fit parameter for all reflections included in the refinement: 0.993
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No