Information card for entry 7012489

Structure parameters

• Formula: C23 H41 N3 Pb Si2
• Calculated formula: C23 H41 N3 Pb Si2
• SMILES: [Pb]12[n]3c(cccc3C=C(N2[Si](C)(C)C)C(C)(C)C)C=C(N1[Si](C)(C)C)C(C)(C)C
• Title of publication: Synthesis and structural characterisation of low-valent Group 14 metal complexes containing tridentate 2,6-pyridyl-bridged bis(1-azaallyl) ligands
• Authors of publication: Leung, Wing-Por; Hou, Henry L.; Cheng, Hui; Yang, Qing-Chuan; Li, Hung-Wing; Mak, Thomas C. W.
• Journal of publication: Dalton Transactions
• Year of publication: 2003
• Journal issue: 8
• Pages of publication: 1505
• a: 9.751 ± 0.002 Å
• b: 12.115 ± 0.002 Å
• c: 12.609 ± 0.003 Å
• α: 103.36 ± 0.03°
• β: 100.73 ± 0.03°
• γ: 100.66 ± 0.03°
• Cell volume: 1382.8 ± 0.6 ų
• Cell temperature: 294 ± 2 K
• Ambient diffraction temperature: 294 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0794
• Residual factor for significantly intense reflections: 0.0734
• Weighted residual factors for significantly intense reflections: 0.2011
• Weighted residual factors for all reflections included in the refinement: 0.2156
• Goodness-of-fit parameter for all reflections included in the refinement: 0.971
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No