Information card for entry 7012620

Structure parameters

• Formula: C10 H13 I4 O2 S
• Calculated formula: C9 H13 Co I3 O Si
• Title of publication: Trimethylsilyl-substituted ligands as solubilizers of metal complexes in supercritical carbon dioxide
• Authors of publication: Francisco Montilla; Vitor Rosa; Chris Prevett; Teresa Avilés; Manuel Nunes da Ponte; Dante Masi; Carlo Mealli
• Journal of publication: Dalton Trans.
• Year of publication: 2003
• Journal issue: 11
• Pages of publication: 2170 - 2176
• a: 6.72 ± 0.003 Å
• b: 9.2099 ± 0.0011 Å
• c: 13.7765 ± 0.001 Å
• α: 88.762 ± 0.008°
• β: 85.443 ± 0.015°
• γ: 71.088 ± 0.017°
• Cell volume: 804 ± 0.4 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0397
• Residual factor for significantly intense reflections: 0.0324
• Weighted residual factors for significantly intense reflections: 0.0872
• Weighted residual factors for all reflections included in the refinement: 0.0912
• Goodness-of-fit parameter for all reflections included in the refinement: 1.119
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: mokα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No