Information card for entry 7012867

Structure parameters

• Formula: C92.25 H105.25 Cl0.75 N O7 P4 Pd4 S3
• Calculated formula: C92.25 H102 Cl0.75 N O7 P4 Pd4 S3
• Title of publication: Synthesis and structural characterisation of the palladium cluster compounds [Pd3(μ-SO2)2(μ-PPh2py)2(PBz3)2] and [Pd4(μ-SO2)2(μ3-S)(CNR)(PBz3)4] (R =tBu, 2,6-dimethylphenyl and cyclohexyl)
• Authors of publication: Anna M. Williamson; Gareth R. Owen; D. Michael P. Mingos; Ramón Vilar; Andrew J. P. White; David J. Williams
• Journal of publication: Dalton Trans.
• Year of publication: 2003
• Journal issue: 12
• Pages of publication: 2526 - 2532
• a: 13.7471 ± 0.0009 Å
• b: 15.2582 ± 0.001 Å
• c: 23.473 ± 0.003 Å
• α: 72.388 ± 0.005°
• β: 85.513 ± 0.008°
• γ: 86.122 ± 0.005°
• Cell volume: 4673.4 ± 0.8 ų
• Cell temperature: 203 ± 2 K
• Ambient diffraction temperature: 203 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0786
• Residual factor for significantly intense reflections: 0.0536
• Weighted residual factors for all reflections: 0.14
• Weighted residual factors for significantly intense reflections: 0.1208
• Goodness-of-fit parameter for all reflections: 1.049
• Goodness-of-fit parameter for significantly intense reflections: 1.095
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No