Information card for entry 7012868

Structure parameters

• Formula: C92.5 H101 N O5.5 P4 Pd4 S3
• Calculated formula: C92.5 H101 N O5.5 P4 Pd4 S3
• Title of publication: Synthesis and structural characterisation of the palladium cluster compounds [Pd3(μ-SO2)2(μ-PPh2py)2(PBz3)2] and [Pd4(μ-SO2)2(μ3-S)(CNR)(PBz3)4] (R =tBu, 2,6-dimethylphenyl and cyclohexyl)
• Authors of publication: Anna M. Williamson; Gareth R. Owen; D. Michael P. Mingos; Ramón Vilar; Andrew J. P. White; David J. Williams
• Journal of publication: Dalton Trans.
• Year of publication: 2003
• Journal issue: 12
• Pages of publication: 2526 - 2532
• a: 13.822 ± 0.003 Å
• b: 15.464 ± 0.004 Å
• c: 23.567 ± 0.007 Å
• α: 71.32 ± 0.02°
• β: 85.57 ± 0.02°
• γ: 87.92 ± 0.014°
• Cell volume: 4757 ± 2 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1446
• Residual factor for significantly intense reflections: 0.089
• Weighted residual factors for all reflections: 0.2663
• Weighted residual factors for significantly intense reflections: 0.2158
• Goodness-of-fit parameter for all reflections: 1.033
• Goodness-of-fit parameter for significantly intense reflections: 1.128
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No