Information card for entry 7012993

Structure parameters

• Formula: C12 H24 Cl2 O4 Pd Te2
• Calculated formula: C12 H24 Cl2 O4 Pd Te2
• SMILES: [Te]12[Pd]([Te](CCOCCOCC1)CCOCCOCC2)(Cl)Cl
• Title of publication: Synthesis and complexation of the mixed tellurium?oxygen macrocycles 1-tellura-4,7-dioxacyclononane, [9]aneO2Te, and 1,10-ditellura-4,7,13,16-tetraoxacyclooctadecane, [18]aneO4Te2 and their selenium analogues
• Authors of publication: Hesford, Matthew J.; Levason, William; Matthews, Melissa L.; Reid, Gillian
• Journal of publication: Dalton Transactions
• Year of publication: 2003
• Journal issue: 14
• Pages of publication: 2852
• a: 10.5109 ± 0.0003 Å
• b: 15.9002 ± 0.0005 Å
• c: 10.9837 ± 0.0003 Å
• α: 90°
• β: 96.8439 ± 0.0011°
• γ: 90°
• Cell volume: 1822.58 ± 0.09 ų
• Cell temperature: 120 ± 0.1 K
• Ambient diffraction temperature: 120 ± 0.1 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.037
• Residual factor for significantly intense reflections: 0.037
• Weighted residual factors for all reflections: 0.047
• Weighted residual factors for all reflections included in the refinement: 0.047
• Goodness-of-fit parameter for all reflections: 1.647
• Goodness-of-fit parameter for all reflections included in the refinement: 1.65
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No