Information card for entry 7013538

Structure parameters

• Common name: Catena-(mu2-O,O'-a,a'-azinobis(4-methoxy-phenyl acetic acid) dimethyl ester)) -tetrakis(mu2-trimethylacetate-O,O') di-rhodium(II,II))
• Chemical name: Catena-(mu2-O,O'-a,a'-azinobis(4-methoxy-phenyl acetic acid) dimethyl ester)) -tetrakis(mu2-trimethylacetate-O,O') di-rhodium(II,II))
• Formula: C40 H56 N2 O14 Rh2
• Calculated formula: C39.88 H55.64 N2 O14 Rh2
• Title of publication: Direct gas-phase interaction of aryldiazoacetates and dirhodium catalystsElectronic supplementary information (ESI) available: 1H NMR spectra for compounds 1 and 2. See http://www.rsc.org/suppdata/dt/b3/b309809p/
• Authors of publication: Petrukhina, Marina A.; Andreini, Kristian W.; Walji, Abbas M.; Davies, Huw M. L.
• Journal of publication: Dalton Transactions
• Year of publication: 2003
• Journal issue: 22
• Pages of publication: 4221
• a: 9.4127 ± 0.0009 Å
• b: 11.7589 ± 0.0011 Å
• c: 12.0273 ± 0.0011 Å
• α: 61.582 ± 0.002°
• β: 76.869 ± 0.002°
• γ: 71.626 ± 0.002°
• Cell volume: 1106.36 ± 0.18 ų
• Cell temperature: 243 ± 2 K
• Ambient diffraction temperature: 243 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0353
• Residual factor for significantly intense reflections: 0.0305
• Weighted residual factors for significantly intense reflections: 0.0756
• Weighted residual factors for all reflections included in the refinement: 0.0782
• Goodness-of-fit parameter for all reflections included in the refinement: 1.047
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No