Information card for entry 7013539

Structure parameters

• Common name: Catena-(mu2-(2,3-bis(4-methoxy-phenyl)-2-Butendioic acid-O,O'- dimethyl ester)-tetrakis(mu2-trifluoroacetato-O,O')- di-rhodium (II,II))
• Chemical name: Catena-(mu2-(2,3-bis(4-methoxy-phenyl)-2-Butendioic acid-O,O'-dimethyl ester)- tetrakis(mu2-trifluoroacetato-O,O')- di-rhodium (II,II))
• Formula: C28 H20 F12 O14 Rh2
• Calculated formula: C28 H20 F12 O14 Rh2
• Title of publication: Direct gas-phase interaction of aryldiazoacetates and dirhodium catalystsElectronic supplementary information (ESI) available: 1H NMR spectra for compounds 1 and 2. See http://www.rsc.org/suppdata/dt/b3/b309809p/
• Authors of publication: Petrukhina, Marina A.; Andreini, Kristian W.; Walji, Abbas M.; Davies, Huw M. L.
• Journal of publication: Dalton Transactions
• Year of publication: 2003
• Journal issue: 22
• Pages of publication: 4221
• a: 10.064 ± 0.003 Å
• b: 20.754 ± 0.006 Å
• c: 8.544 ± 0.002 Å
• α: 90°
• β: 107.01 ± 0.004°
• γ: 90°
• Cell volume: 1706.5 ± 0.8 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0681
• Residual factor for significantly intense reflections: 0.0521
• Weighted residual factors for significantly intense reflections: 0.1056
• Weighted residual factors for all reflections included in the refinement: 0.1105
• Goodness-of-fit parameter for all reflections included in the refinement: 1.285
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No