Information card for entry 7013858

Structure parameters

• Formula: C12 H12 Cl3 Ge P
• Calculated formula: C12 H12 Cl3 Ge P
• SMILES: [Ge](Cl)(Cl)[Cl-].[PH2+](c1ccccc1)c1ccccc1
• Title of publication: The reaction of GeCl4 with primary and secondary phosphines.
• Authors of publication: Apostolico, Leonardo; Mahon, Mary F.; Molloy, Kieran C.; Binions, Russell; Blackman, Christopher S.; Carmalt, Claire J.; Parkin, Ivan P.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2004
• Journal issue: 3
• Pages of publication: 470 - 475
• a: 10.276 ± 0.0002 Å
• b: 14.492 ± 0.0003 Å
• c: 10.305 ± 0.0002 Å
• α: 90°
• β: 103.653 ± 0.0009°
• γ: 90°
• Cell volume: 1491.25 ± 0.05 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0553
• Residual factor for significantly intense reflections: 0.0337
• Weighted residual factors for significantly intense reflections: 0.0727
• Weighted residual factors for all reflections included in the refinement: 0.0807
• Goodness-of-fit parameter for all reflections included in the refinement: 1.023
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No