Information card for entry 7013859

Structure parameters

• Formula: C6 H14 Cl3 Ge P
• Calculated formula: C6 H14 Cl3 Ge P
• SMILES: [Ge](Cl)(Cl)[Cl-].[PH3+]C1CCCCC1
• Title of publication: The reaction of GeCl4 with primary and secondary phosphines.
• Authors of publication: Apostolico, Leonardo; Mahon, Mary F.; Molloy, Kieran C.; Binions, Russell; Blackman, Christopher S.; Carmalt, Claire J.; Parkin, Ivan P.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2004
• Journal issue: 3
• Pages of publication: 470 - 475
• a: 30.2955 ± 0.0009 Å
• b: 6.1385 ± 0.0002 Å
• c: 12.9839 ± 0.0005 Å
• α: 90°
• β: 103.999 ± 0.001°
• γ: 90°
• Cell volume: 2342.89 ± 0.14 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0496
• Residual factor for significantly intense reflections: 0.0329
• Weighted residual factors for significantly intense reflections: 0.0766
• Weighted residual factors for all reflections included in the refinement: 0.0845
• Goodness-of-fit parameter for all reflections included in the refinement: 1.01
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No