Information card for entry 7013880

Structure parameters

• Common name: (P4(P(NiPr2)(N(SiMe3)2))2)
• Formula: C24 H64 N4 P6 Si4
• Calculated formula: C24 H64 N4 P6 Si4
• Title of publication: Synthesis and P-P cleavage reactions of [P(X)X']2; X-ray structures of [Co[P(X)X'](CO)3] and P4[P(X)X']2[X = N(SiMe3)2, X'= NPri2].
• Authors of publication: Bezombes, Jean-Philippe; Hitchcock, Peter B.; Lappert, Michael F.; Nycz, Jacek E.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2004
• Journal issue: 4
• Pages of publication: 499 - 501
• a: 13.8004 ± 0.0007 Å
• b: 11.0049 ± 0.0005 Å
• c: 14.7827 ± 0.0007 Å
• α: 90°
• β: 112.336 ± 0.002°
• γ: 90°
• Cell volume: 2076.63 ± 0.17 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 7
• Hermann-Mauguin space group symbol: P 1 a 1
• Hall space group symbol: P -2ya
• Residual factor for all reflections: 0.0587
• Residual factor for significantly intense reflections: 0.0495
• Weighted residual factors for significantly intense reflections: 0.1207
• Weighted residual factors for all reflections included in the refinement: 0.1273
• Goodness-of-fit parameter for all reflections included in the refinement: 1.037
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No