Crystallography Open Database

Information card for entry 7013885

Preview

Coordinates	7013885.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C56 H96 B5 O6 P4 Rh
Calculated formula	C56 H96 B5 O6 P4 Rh
SMILES	[Rh]([P](CC)(CC)CC)([P](CC)(CC)CC)([P](CC)(CC)CC)[P](CC)(CC)CC.O1[B]2(OB(OB1c1c(cccc1C)C)c1c(cccc1C)C)OB(OB(O2)c1c(cccc1C)C)c1c(cccc1C)C
Title of publication	Cationic Rh complexes with novel spiro tetraarylpentaborate anions prepared from arylboronic acids and aryloxorhodium complexes.
Authors of publication	Nishihara, Yasushi; Nara, Kyoko; Nishide, Yasuhiro; Osakada, Kohtaro
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2004
Journal issue	9
Pages of publication	1366 - 1375
a	14.3 ± 0.003 Å
b	27.509 ± 0.006 Å
c	16.606 ± 0.005 Å
α	90°
β	93.23 ± 0.02°
γ	90°
Cell volume	6522 ± 3 Å³
Cell temperature	296.1 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for significantly intense reflections	0.056
Weighted residual factors for all reflections included in the refinement	0.067
Goodness-of-fit parameter for all reflections included in the refinement	1.004
Diffraction radiation wavelength	0.7107 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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