Information card for entry 7013886

Structure parameters

• Formula: C33 H34 O P Rh
• Calculated formula: C33 H34 O P Rh
• SMILES: [Rh]123([P](c4ccccc4)(c4ccccc4)c4ccccc4)(Oc4ccc(cc4)C)[CH]4=[CH]1CC[CH]2=[CH]3CC4
• Title of publication: Cationic Rh complexes with novel spiro tetraarylpentaborate anions prepared from arylboronic acids and aryloxorhodium complexes.
• Authors of publication: Nishihara, Yasushi; Nara, Kyoko; Nishide, Yasuhiro; Osakada, Kohtaro
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2004
• Journal issue: 9
• Pages of publication: 1366 - 1375
• a: 11.918 ± 0.003 Å
• b: 12.525 ± 0.002 Å
• c: 9.851 ± 0.002 Å
• α: 106.79 ± 0.01°
• β: 90.22 ± 0.02°
• γ: 79.76 ± 0.02°
• Cell volume: 1383.6 ± 0.5 ų
• Cell temperature: 23 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for significantly intense reflections: 0.03
• Weighted residual factors for all reflections included in the refinement: 0.043
• Goodness-of-fit parameter for all reflections included in the refinement: 0.95
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No